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 For the first time, a versatile electrolyte bath is described that can be used to electrodeposit a wide range of p block elements from supercritical difluoromethane (scCH2F2). The bath comprises the tetrabutylammonium chlorometallate complex of the element in an electrolyte of 50 10'3 mol dm'3 tetrabutylammonium chloride at 17.2 MPa and 358 K. Through the use of anionic ([GaCl4]', [InCl4]', [GeCl3]', [SnCl3]', [SbCl4]', and [BiCl4]') and dianionic ([SeCl6]2' and [TeCl6]2') chlorometallate salts, the deposition of elemental Ga, In, Ge, Sn, Sb, Bi, Se, and Te is demonstrated.


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